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In this study, we present the solvothermal synthesis of LuPO4:Pr3+ (1%) nanocrystals in a dimethyl sulfoxide-water solvent system. The as-prepared nanocrystals exhibit a relatively high degree of crystallinity, along with significant short-range disorder, particularly in the anionic sublattice, as revealed by XRD and Raman spectroscopy data. Low temperature luminescence spectroscopy under VUV exci
